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An improved hydrothermal diamond anvil cell
Li, Jiankang1; Bassett, W. A.2; Chou, I-Ming3; Ding, Xin4; Li, Shenghu3; Wang, Xinyan4
2016-06-01
Source PublicationREVIEW OF SCIENTIFIC INSTRUMENTS
Volume87Issue:5
AbstractA new type of HDAC-V hydrothermal diamond anvil cell (HDAC-VT) has been designed to meet the demands of X-ray research including X-Ray Fluorescence, X-ray Absorption Spectroscopy, and small angle X-ray scattering. The earlier version of HDAC-V that offered a large rectangular solid angle used two posts and two driver screws on both sides of a rectangular body. The new version HDAC-VT in a triangular shape has two alternative guide systems, either three posts inserted into bushings suitable for small anvil faces or linear ball bearings suitable for large anvil faces. The HDAC-VT having three driver screws offers the advantage of greater control and stability even though it sacrifices some of the size of solid angle. The greater control allows better sealing of samples, while greater stability results in longer survival for anvils and ceramic parts. This improved design retains several beneficial features of the original HDAC-V as well. These include the small collar that surrounds the heater and sample chamber forming an Ar + H-2 gas chamber to protect diamonds and their heating parts from being oxidized. Three linear ball bearings, when used, fit to the three posts prevent seizing that can result from deterioration of lubricant at high temperatures. Positioning the posts and bearings outside of the gas chamber as in HDAC-V also prevents seizing and possible deformation due to overheating. In order to control the heating rate precisely with computer software, we use Linkam T95 and have replaced the Linkam 1400XY heating stage with the HDAC-VT allowing the HDAC to be heated to 950 degrees C at a rate from 0.01 degrees C/min to 50 degrees C/min. We have used the HDAC-VT and Linkam T95 to observe in situ nucleation and growth of zabuyelite in aqueous fluid and to homogenize melt inclusions in quartz from three porphyry deposits in Shanxi, China. Published by AIP Publishing.
SubtypeArticle
WOS HeadingsScience & Technology ; Technology ; Physical Sciences
DOI10.1063/1.4947506
URL查看原文
Indexed BySCI
Language英语
WOS KeywordRARE-EARTH-ELEMENTS ; AQUEOUS-SOLUTIONS ; FLUID INCLUSIONS ; SUPERCRITICAL CONDITIONS ; CHLORO COMPLEXES ; MELT INCLUSIONS ; SILICATE MELT ; PEGMATITES ; STABILITY ; AQUA
WOS SubjectInstruments & Instrumentation ; Physics, Applied
WOS IDWOS:000379187600028
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Cited Times:1[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Version同行评议接收稿
Identifierhttp://ir.idsse.ac.cn/handle/183446/1538
Collection深海科学研究部_深海极端环境模拟研究实验室
Affiliation1.Chinese Acad Geol Sci, Inst Mineral Resources, MLR Key Lab Metallogeny & Mineral Assessment, Beijing 100037, Peoples R China
2.Cornell Univ, Dept Earth & Atmospher Sci, Ithaca, NY 14853 USA
3.Chinese Acad Sci, Sanya Inst Deep sea Sci & Engn, Sanya 572000, Hainan, Peoples R China
4.China Univ Geosci Beijing, Beijing 100083, Peoples R China
Recommended Citation
GB/T 7714
Li, Jiankang,Bassett, W. A.,Chou, I-Ming,et al. An improved hydrothermal diamond anvil cell[J]. REVIEW OF SCIENTIFIC INSTRUMENTS,2016,87(5).
APA Li, Jiankang,Bassett, W. A.,Chou, I-Ming,Ding, Xin,Li, Shenghu,&Wang, Xinyan.(2016).An improved hydrothermal diamond anvil cell.REVIEW OF SCIENTIFIC INSTRUMENTS,87(5).
MLA Li, Jiankang,et al."An improved hydrothermal diamond anvil cell".REVIEW OF SCIENTIFIC INSTRUMENTS 87.5(2016).
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